Lesson 8 of the Profex workshop at the Forschungszentrum Jülich, Germany, in March 2024 discusses some common refinement challenges. The first example provides information about how texture / preferred orientation is refined in Profex. The second example demonstrates how to refine anisotropic crystallite sizes. The third example shows how to create electron density maps (difference Fourier maps), and how they can help with structure refinements.
Slides and example files are avialable for download on
https://www.profex-xrd.org
Profex workshops are kindly supported by RMS Foundation, Switzerland:
https://www.rms-foundation.ch
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https://www.youtube.com/watch?v=0_0uqdPQTU4
When upgrading from Profex 4.1 or older to version 4.2 or newer, adding and indexing new structure files may no longer work. But the solution is simple...
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https://www.youtube.com/watch?v=UqBtPYgMk8E
In part 1 of this case study I am creating a Profex instrument configuration for a PANalytical Empyrean diffractometer.
01:22 Creating the refinement project
03:24 Adapting the instrument configuration
14:39 Changing the radiation spectrum
20:53 Saving the configuration to the device repository
Visit the Profex website:
https://www.profex-xrd.org
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https://www.youtube.com/watch?v=ZO_LmaShrAw
This is a quick summary of the new features in Profex version 4.3.4, as well as a presentation of the new waterfall plot dialog.
Credits for the waterfall picture in the thumbnail:
"Kirkjufellsfoss Waterfall" by Mustang Joe is marked with CC0 1.0
Visit the Profex website:
https://www.profex-xrd.org
Profex Tutorials on Odysee:
https://odysee.com/@ProfexTutorials:2
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https://www.youtube.com/watch?v=-SKgICrI7IU
I am presenting Profex version 5.0.0, the latest major release with new features and support for the Apple Silicon platform.
Visit the Profex website:
https://www.profex-xrd.org
Profex Tutorials on Odysee:
https://odysee.com/@ProfexTutorials:2
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https://www.youtube.com/watch?v=xD2plEdYRfg
Profex version 4.3 comes with a new feature: The COD database can be searched directly, and CIF files can be imported and converted to the STR format very easily.
This video shows how to install the COD database and how to set up Profex accordingly.
Visit the Profex website:
https://www.profex-xrd.org
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https://www.youtube.com/watch?v=3AdXsogfQEg
In this tutorial I demonstrate how to control refinement of the background curve in Profex.
02:31 Changing the number of background coefficients
04:50 Measured backgrounds
08:40 Amorphous peaks
Visit the Profex website:
https://www.profex-xrd.org
Profex tutorials mirror on Odysee.com:
https://odysee.com/@ProfexTutorials:2
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https://www.youtube.com/watch?v=Bo2nwEni6dc
We delve into Rietveld refinement of isotropic and anisotropic crystallite sizes, as well as texture / preferred orientation with Profex and BGMN.
Download the example file:
https://www.profex-xrd.org/wp-content/uploads/2021/01/ex2-file1.zip
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https://www.youtube.com/watch?v=dGM_q6mlALM