We show how to make hydrobromic acid.
Hydrobromic acid is the bromine analogue of hydrochloric acid. While too expensive to use as much as hydrochloric acid, it's often used when the bromine element itself is needed. For example a major use is the synthesis of organobromine compounds like the ones we used in our grignard reactions.
To make it, we start with 400mL of water and add to it 250g of sodium bromide. Sodium bromide is available as a bromine source for swimming pools. To this we add 200mL of sulfuric acid, I got mine from drain opener.
The mixture is stirred until everything is dissolved and then cooled to freezing to crystallize out the byproduct sulfates and bisulfates.
The filtrate is then distilled until half the volume has been transferred and then allowed to cool. More crystals should crash out. This is filtered again and the filtrate is again distilled.
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https://www.youtube.com/watch?v=4ei_xUIhRas
In this video we make ammonia gas and dissolve it water from various chemicals easily accessible to the amateur.
The first method is merely boiling household ammonia solution that's domestically available from the local supermarket. The ammonia boiled out is lead into cold water where it can be dissolved. While this did work the yield was quite low at around 2.5g per 100mL of household ammonia solution. From the 600mL of ammonia solution used only about 15g was obtained.
The second method was to revisit the classic method to produce sodium nitrate from ammonium nitrate and sodium hydroxide by dissolving them both separately in water and then mixing them together and trying to boil out the ammonia. This worked terribly and i got almost no yield at all.
The third method that seemed to work the best was to react urea and sodium hydroxide in water. This reaction was well-behaved, steady and easily performed with domestically available chemicals. Starting from 200mL water, 90g urea and 120g sodium hydroxide, about 38.6g of ammonia was obtained.
I intend to use the ammonia in a future project to make nitric acid.
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https://www.youtube.com/watch?v=0-jJ5QF-EVE
In this video we make a chemical thunderstorm in a beaker using manganese heptoxide.
I wanted recreate the test tube thunderstorm on a larger scale, adding sound for a more immersive experience. The setup involved using a glass funnel to carefully pour sulfuric acid into ethanol and form a layer of it in the bottom. Sprinkling potassium permanganate into the mix led to the formation of manganese heptoxide that reacted with ethanol and produced display of small explosions, accompanied by popping sounds and flashes of light.
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In this video we do something really silly and remove a can from the coke it contains.
To do the demonstration: First get any soft drink can and using sandpaper, sand off the label. Then open the can and suspend it by the tab in 5% hydrochloric acid. The exact concentration is not critical. The can must be opened or it will rupture as the aluminum is removed.
over the course of an hour, the aluminum in the can will be attacked by the acid and dissolve away. This leaves behind the drink and also a very thin plastic liner inside the can. This liner protects the drink from leaching metals out of the can. Carefully lift the can to reveal the liner still holding the drink.
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In this video we purify and concentrate dilute nitric acid using a combination of fractional distillation and drying agents to produce azeotropic nitric acid and fuming nitric acid.
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In this video we construct and demonstrate a Dean-Stark trap. A very useful piece of equipment when distilling azeotropic mixtures of immisicble liquids.
This video has been generously supported by the following sponsors:
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https://www.youtube.com/watch?v=jxgpLp279Yc
In this video we make sulfuric acid by the copper chloride process.
The general idea is simple: Take a solution of copper (II) chloride and bubble sulfur dioxide into it until most of the copper (II) chloride is converted into copper (I) chloride. This reaction also converts the sulfur dioxide into sulfuric acid and produces hydrochloric acid. Now the copper chloride can be regenerated by bubbling air into the mixture until the copper chloride dissolves again. This cycle can be repeated. When you want to isolate the sulfuric acid you forgo air infusion for that step and filter off the preciptated copper chloride. Then you distill off the hydrochloric acid and water from the filtrate. The sulfuric acid left behind will precpitate out most of the remainig copper salts and when filtered will give you relatively pure sulfuric acid with some water and minor copper contamination. The copper chloride can be recombined with all the hydrochloric acid from before and the cycle repeated.
Related videos:
Make a heating mantle to distill sulfuric acid: https://www.youtube.com/watch?v=N5meDWAqYes
Distilling sulfuric acid: https://www.youtube.com/watch?v=tgUH0HXrOKE
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https://www.youtube.com/watch?v=l2AkVYxDSKc
We show how to purify aluminum nitrate and strontium nitrate by recrystallization. This is important because those two substances must be extremely pure for our upcoming video on making glow in the dark powder.
First make aluminum nitrate from our previous video: http://www.youtube.com/watch?v=u4Ha1SJrazY
Dissolve the dry aluminum nitrate in water and filter off any insoluble materials. We could not filter it off before it dried in the previous video because the particles at that stage are much too small. It needs crystallize once to aggregate into particles large that can be filtered.
After filtering, dry off the aluminum nitrate. The desiccator bag might be useful here: http://www.youtube.com/watch?v=XJFfS_YbbYI
After drying, carefully weigh out the crystals. Then take that mass and add in 20% mass of water. So if you have 50g like me, you add 10g of water (or 10mL since density is 1g/mL).
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https://www.youtube.com/watch?v=uVA0rK_VITY