Synthesis of A Very Rare Compound: Thallium(I) Perrhenate
In this video prepare the exotic compound thallium(I) perrhenate; the least water soluble perrhenate compound of the type M(I)ReO4 where M(I) is a Li, Na, K, Rb, Cs, Ag, or Tl monovalent cation. This chemical curiosity is one of the heaviest compounds I've ever seen. Despite it being a very fine powder it will settle out of a suspension in water almost completely in less than a minute. It has no practical uses that I am aware of.
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In this video I prepare an ammine complex of palladium dichloride. Unfortunately I ended up adding way too much ammonia which complicated this otherwise simple prep. After getting some help to know how to go about solving this problem I was able to complete the prep with no issues.
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In this video I demonstrate a lead dioxide based thermite so that people can see this apparently legendary thermite reaction. Here at the Poor Mans Chemist we strive to give the public what it wants. I was hoping for something a bit more explosive but this run of the mill thermite reaction is all I got. There were no casualties.
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Please consider supporting this channel! Thank you! :-) In this real time video I demo a mix of chems so powerful that it completely dissolved a 16.53 gram tungsten rod in about 4 minutes. This mix of chems is a molten 1:1 mix of potassium nitrate and potassium hydroxide and it's so strong that virtually no metal can withstand it.
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In this video I first prepare palladium dicyanide from palladium dichloride dihydrate and sodium potassium cyanide NaK2(CN)3 (the sodium potassium cyanide was prepared in the normal way from sodium metal and anhydrous potassium ferrocyanide). I then centrifuged off the Pd(CN)2 precipitate and after suspending it in water converted it to the tetracyanopalladate(II) complex by addition of more cyanide. Some fraction of the product is actually sodium potassium tetracyanopalladate(II) but what can you do?
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In this video we cover the synthesis of alkenes from alcohols as well as the phenomena of molecular rearrangements which can be a complete pain in many syntheses (unless the predominant rearrangement product is what you're after of course). We also begin to cover the vic and gem dihalides and the synthesis of alkynes.
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In this video I prepare niobium pentabromide and the oxytribromide from niobium and bromine in an atmosphere of CO2.
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In this video I prepare barium sulfide from iron, sulfur, and barium hydroxide octahydrate. There were some hiccups along the way but in the end I was able to get a good product that seems to be largely free of barium carbonate.
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In this video I attempt to synthesize RbPbI3.2H2O. Whether it actually worked or not isn't very clear. I think it probably worked which is why it made the cut to be a video but I would greatly value any feedback y'all might be able to provide!!
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In this video I try dissolving gold in selenic acid and H2O2 and fail. However, addition of a small amount of bromine resulted in the gold dissolving in minutes. After evaporation of the bromine out of solution a red liquid was obtained from which a yellow solid crystallized. This may have been gold(III) selenate. However, further attempts to dissolve these crystals and evaporate the solution further resulted in decomposition of the solution with the precipitation of what I suspect is metallic gold. However, not ALL the gold can have precipitated. There simply isn't enough of it. The final product obtained was a bright red solution which I suspect is a small amount of gold(III) selenate dissolved in selenic acid.
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