Making Old Timey White Colored Fire Using Arsenic (Realgar)
In this video I try using arsenic to color a flame white as was done in the days before things like powdered aluminum. This mix produces arsenic trioxide laden smoke so it should not be repeated by anyone.
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In this video I prepare the interhalogen compound iodine monobromide from equimolar amounts of elemental bromine (10 grams) and elemental iodine (15.88 grams). IBr is an interesting compound since the iodine bears a partial positive charge and the bromine a partial negative carge. IBr is used to cleave carbon-metal bonds to produce organic iodides and metal bromides. It is also used to convert alkenes into vicinal bromoiodides, effect the electrophilic cyclization of homoallylic carbonates, and alpha-bromination of steroidal aldehydes and ketones. IBr has also been used for brominating phenol and aryl ether derivatives. (Information taken from the Encyclopedia of Reagents for Organic Sythesis).
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In this video the extremely problematic camera that I have been using up until recently that could never focus properly gets the fiery justice it so richly deserves.
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I made some cesium chlorate to use in an experiment recently and I discovered that it was still contaminated with a fair bit of sodium. So I decided to recrystallize it and try filming it to see if it would look cool or not (not everything does). Happily it rated pretty high on the coolness index to I decided to share it with everyone else. Hope you enjoy it!
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In this video I prepare a cyanide complex of silver that has historically been used in silver plating.
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In this video I prepare dinitrotetramminenickel(II) from nickel(II) chloride hexahydrate. This synthesis could also begin with nickel(II) carbonate or nickel(II) acetate although if beginning with the acetate some acetic acid should still be added to prevent hydrolysis (according to the textbook anyways).
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My first successful prep of the highly exotic and extremely poisonous thallous cyanide. This prep should only be attempted by experienced amateur and professional chemists with good lab technique. TlCN is used in organic synthesis.
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In this video I prepare an ammine complex of palladium dichloride. Unfortunately I ended up adding way too much ammonia which complicated this otherwise simple prep. After getting some help to know how to go about solving this problem I was able to complete the prep with no issues.
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I prepare fulminating gold from chloroauric acid and from that I make potassium dicyanoaurate(I) by addition of aqueous sodium potassium cyanide solution. After crystallization of the K[Au(CN)2] (got a good timelapse!) the dicyanoaurate(I) is reacted with concentrated HCl and heated. This precipitates out aurous cyanide AuCN. The Handbook of Preparative Inorganic Chemistry said that moist AuCN was photosensitive to sunlight but that does not appear to extend to the compound under water (at least not in the short term)
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In this video I make up a few uranyl compounds as described on atomistry. We start with making thallium uranyl carbonate followed by uranyl hypophosphite which I then turn into uranyl metaphosphate.
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