In this video I demonstrate a lead dioxide based thermite so that people can see this apparently legendary thermite reaction. Here at the Poor Mans Chemist we strive to give the public what it wants. I was hoping for something a bit more explosive but this run of the mill thermite reaction is all I got. There were no casualties.
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In this video we wrap up Chapter 3. We discuss the acidity of phenols and phenoxide ions, the effects of solvent on acidity, oxonium ions, a detailed discussion of the reaction of HCl with t-butanol to produce t-butyl chloride (2-chloro-2-methylpropane), acid and bases in non-aqueous solvents, alkyllithiums, and deuterium/tritium labeling of organic compounds.
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In this video I begin to cover nucleophilic substitution reactions; specifically SN2 reactions. We begin with a discussion of the extremely useful alkyl halides and then move on to nucleophiles, leaving groups, SN2 reaction kinetics, before concluding with a discussion of the mechanism for SN2 reactions.
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In this video I make silver chlorite from sodium chlorite and silver nitrate. I then demonstrate how unstable this compound is and how it will explode on percussion when mixed with sulfur. Silver chlorite reacts explosively with a number of other substances and all in all is a pretty dangerous (but also really fun) compound.
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Thallium sulfate was prepared by dissolving thallium metal into 1.5M sulfuric acid to which a small amount of HNO3 was added. The solution was evaporated until the thallium sulfate crystallized.
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Niobium metal reacts with molten KOH to produce potassium niobate and hydrogen gas. The melt is so hot that the hydrogen bubbles exploded on contact with air.
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In this very short video I show you my first test of an old mix used to create a purple colored flame. The mixture contains potassium chlorate, calomel, strontium nitrate, and cupric oxide. The original formulation also called for shellac but both it and its popular substitute (red gum) were sold out on Fireworks Cookbook. So I tried it with gum arabic instead. Clearly that was a bad choice. But this experiment confirms that I am on the right track to achieving a pure purple flame and what I learned from the attempt will allow me to formulate a mix that burns continuously. Not knowing what the smoke contains I am going overboard with the safety on this one and will only do the second attempt when the wind is blowing back towards the woods consistently and it's late at night so there is no chance whatsoever of anyone being in any danger at all.
Composition Recipe at Fireworks Cookbook:
https://fireworkscookbook.com/firework-recipe/g-w-purple-pill-box-chlorate/
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New video. While tinkering with the reaction between sodium and tellurium I stumbled across a way to slow the reaction down and actually produce a decent amount of sodium telluride. Normally this combination of the elements just explodes much like the combination of sodium and sulfur which is the lighter congener of tellurium.
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In this video we cover electrophilic addition of halogens and hydrogen halides to alkenes and alkynes, the prep of halohydrins, the synthesis of cyclopropanes (carbenes and carbenoids), syn 1,2-hydroxylation, and the oxidative cleavage of alkenes and alkynes by ozonolysis and KMnO4.
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Cyclopropanes From an Easily Prepared Highly Active Zinc-Copper Couple, Diiodomethane, and Olefins
DOI: 10.1021/jo01030a529
Paper on SciHub: https://sci-hub.se/10.1021/jo01030a529
In this video I prepare rubidium hexabromothallate starting with aqueous thallium(I) sulfate. This preparation comes from the Handbook of Preparative Inorganic Chemistry page 876.
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